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Oxidative Cyclization lntramolecular disulfide bridge formation between the cysteine residues at positions 2 and 7 (initially coupled as acetamidomethyl (Acm)-protected cysteine) was performed with the peptide still attached to the resin, using 163 mg of thallium(III) trifluoroacetate (Tl(TFA) 3 ) in 5 mL of N -methyl-2-pyrrolidone (NMP) in a simultaneous Acm deprotection and disulfide-formation step
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